Very popular advice. It makes sense from the point of chemistry, but if we ask a question "how long is it going to take", it is rarely useful.
I’ll refrain from quoting the rest of your long and detailed reply,
Leonid, but will say that I’ve broken my fair share of bits, exactly
as you describe, in metal just as thick, sometimes thicker. Typical
broken drills will be dissolved via my described method in anywhere
from 15 minutes to an hour, depending on just how much metal is
there. Almost never takes longer than that. The times you descirbe,
I’d agree would be too long. Overnight? If it took that long, I too
would be reaching for the centerpunch. Another trick I’ve sometimes
used is with the laser welder. Set to high power, very tight focus
(small spot), and a very short pulse length, the laser makes a
halfway decent drill for imprecise pilot holes. Useful for blasting
out bits of remaining ceramic-hard platinum casting investment too,
which otherwise destroys bits. Anyway, with the drill bits, blast
through the hole with the laser. This welds steel to your metal too,
which isn’t desired. But then the pickle gets the job done faster,
removing the steel and leaving a pilot hole. However, though this
method can be useful, generally, I use it only when I suspect
something hard (like that investment inclusion) was the cause of the
breakage. Otherwise, I just let the pickle do it’s thing. And as I
say, it doesn’t seem to take as long for me, as you seem to have
experienced. Try mixing up the pickle stronger, and be sure it’s
hot.
Note that I mix the pickle solution fairly strong. While still cold,
a tiny drop on a fingertip, tasted, will be uncomfortably sour
tasting, but won’t actually burn. (and yes, this is reasonably safe
to do. spit it out and rinse, and you’re fine. Don’t do this with
electroplating solutions, of course… ) I know that’s not an
accurate recipe of how strong to mix it, but it’s a useful quick
check.
As well, for removing drill bits, the solution is boiling, or almost
so. You can speed it up even more by suspending the beaker with hot
pickle in an ultrasonic cleaner. That can cut the time in half, as
ultrasonic cleaners concentrate their activity in holes, greatly
increasing the aggressiveness of the acid attack on the steel.
Cheers
Peter